In British Pharmacopoeia (BP) assay for content of active ingredient, 20 tablets
(each stated to contain 50 mg of active ingredient) of total weight 6.5142g were
powdered. A sample of the powdered tablets of weight 0.3460g was extracted
with 0.1M NaOH, the extract filtered, and the filtrate made up to 100 cm3 with
0.1 M NaOH. A dilution ( 1 in 100 ) with 0.1M NaOH gave an absorbency value
of 0.345 at 256 nm using 1 cm cells. Given that the A (1%, 1cm) is 658 at 257 nm
in 0.1M NaOH. Calculate the percentage of the stated amount of active
ingredient per tablet

Question

04-06-2022
Medicine

Answered

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In British Pharmacopoeia (BP) assay for content of active ingredient, 20 tablets
(each stated to contain 50 mg of active ingredient) of total weight 6.5142g were
powdered. A sample of the powdered tablets of weight 0.3460g was extracted
with 0.1M NaOH, the extract filtered, and the filtrate made up to 100 cm3 with
0.1 M NaOH. A dilution ( 1 in 100 ) with 0.1M NaOH gave an absorbency value
of 0.345 at 256 nm using 1 cm cells. Given that the A (1%, 1cm) is 658 at 257 nm
in 0.1M NaOH. Calculate the percentage of the stated amount of active
ingredient per tablet

Sagot :

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